Technical Information

1 Short Application Note on Sheet Resistance, Ohms-Per-Square, and the Calculation of Resistivity or Thickness

2 Basic information regarding how to make four point probe measurements using Jandel resistivity test equipment.

3 Four Point Probe Theory - A helpful article

4 Four Point Probe Equations - A helpful article from the      University of Illinois - Urbana/Champaign

5 Understanding volume resistivity measurements and converting between ohms-per-square (sheet resistance) and ohms-cm (volume resistivity)

6 Sample Size Requirements and Correction Factors Some questions and answers from Jandel Engineering Ltd.

7 Haldor Topsoe Technical Documents Regarding Correction Factors Correction Factor for various material shapes and sizes

8 1964 National Bureau of Standards Technical Note 199, "Correction Factor Tables for Four-Point Probe Resistivity Measurements on Thin, Circular Semiconductor Samples"

9 Finite-Size Corrections for 4-Point Probe Measurements, by J. R. Senna, Instituto Nacional de Pesquisas Espaciais (INPE), Brasil

10 Questions and answers re: resistivity & resistance, sheet resistance, volume resistivity, surface resistivity by John Clark of Jandel Engineering

11 Q & A regarding the use of Jandel Resistivity Measurement equipment by Pete Clark of Jandel Engineering

12 Four-Point Probe Theory of Operation from the University of California, Berkeley, EECS web site (PDF file)

13 A table of suggested probe tip specifications for various silicon wafer types.

14 A table of common four point probe tip radii and spacings

15 Osmium alloy tips versus tungsten carbide tips

16 Square array versus linear array four point probe

17 Reversing current to check the validity of a 4 point probe measurement

18 Determining the best choice of probe tip specifications (tip spacing, spring loads, material, radii) for a given material.

19 What is the expected life of a Jandel Four Point Probe Head?

20 Jandel FAQ

Hall Effect Measurement Technical info:

21 Wikipedia article regarding the Hall Effect

22 Wikipedia article regarding the Van der Pauw method

23 NIST web page regarding the theory and implementation of the Hall Effect Measurement technique

 

EECS 143 Microfabrication Technology

Four-Point Probe Manual

1. Introduction

 

The purpose of the 4-point probe is to measure the resistivity of any semiconductor material. It can measure either bulk or thin film specimen, each of which consists of a different expression. The derivation will be shown in this tutorial.

 

The 4-point probe setup used in the EECS 143 instructional lab consists of four equally spaced tungsten metal tips with finite radius. Each tip is supported by springs on the other end to minimize sample damage during probing. The four metal tips are part of an auto-mechanical stage which travels up and down during measurements. A high impedance current source is used to supply current through the outer two probes; a voltmeter measures the voltage across the inner two probes (See Figure 1) to determine the sample resistivity. Typical probe spacing s ~ 1 mm.

 

Figure 1. Schematic of 4-point probe configuration

Figure 1. Schematic of 4-point probe configuration

 

 

2. Theory

 

  1. Bulk Sample

     

    In our derivations for this section, we assume that the metal tip is infinitesimal and samples are semi-infinite in lateral dimension. For bulk samples where the sample thickness t >> s, the probe spacing, we assume a spherical protrusion of current emanating from the outer probe tips. The differential resistance is:

    We carry out the integration between the inner probe tips (where the voltage is measured):

    where probe spacing is uniformly s. Due to the superposition of current at the outer two tips, R = V/2I. Thus, we arrive at the expression for bulk resistivity:

  2. Thin Sheet

     

    For a very thin layer (thickness t << s), we get current rings instead of spheres. Therefore, the expression for the area . The derivation is as follows:

     

    Consequently, for R = V/2I, the sheet resistivity for a thin sheet is:

     

    Note that this expression is independent of the probe spacing s. Furthermore, this latter expression is frequently used for characterization semiconductor layers, such as a diffused N+ region in a p-type substrate. In general, the sheet resistivity can be expressed as:

     

    where the factor k is a geometric factor. In the case of a semi-infinite thin sheet, k = 4.53, which is just from the derivation. The factor k will be different for non-ideal samples.

 

 

3. Operation Procedures

 

The following steps should be taken in the following sequence:

 

  1. Turn on the voltmeter, set the mode to DC and voltage range to 200 mV.
  2. Place wafer onto the probe stage.
  3. Flip the toggle switch located atop the probe station from "NEUTRAL" TO "DOWN".
  4. Watch the probe casing lower until the probes stabilize on the wafer.
  5. Return the toggle switch of the probe station to the "NEUTRAL" position.
  6. Turn on the current source by turning the black switch "S1" to the "ON" position.
  7. Set the current to the desired level, and proceed with measuring the voltage across the inner two probes. Map the wafer.
  8. When measurement is finished, shut off the current source by turning the switch "S1" to the "OFF" position.
  9. Flip the probe station toggle switch from "NEUTRAL" to "UP".
  10. Wait until the probe casing is all the way up, then set the toggle switch back to "NEUTRAL".
  11. Turn off voltmeter.

 

James Chan, Spring 1994

The original page can be found here: http://microlab.berkeley.edu/ee143/Four-Point_Probe/

 

 


Four-Point-Probes is a division of Bridge Technology. To request further information please call Bridge Technology at (480) 988-2256 or send e-mail to Larry Bridge at: sales@bridgetec.com